Methamphetamine synthesis from P2P by NaBH4 reduction. Medium-Scale.

Maya

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Purity of this method?
What means DCM
 

btcboss2022

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From 966gr clean P2P I got 950gr of Meth oil
From 966gr of "dirty" P2P I got 800gr of Meth oil.
 

btcboss2022

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DCM is Dicloromethane
 

G.Patton

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88.4% good yield (y)
 

Phoneix73

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is methamphetamine oil normal crystal methamphetamine
 

btcboss2022

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btcboss2022

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Here is the final ICE meth from the oil:

IWjPOKZNd3
 
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hustlerkid

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Did you separate D&L before crystal?
 

Win Win

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Hi sir. You follow this recipe? Can you teach me?
 

Maya

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But it will melt
 

Maya

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What alternative of this
 

btcboss2022

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Ether, toluene....
 

btcboss2022

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Bartholomeus

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Very nice crystal cake :)
When you have final dry weight in grams please update with it, I have interest in seeing how much dry you got from 950ml of meth oil
 

btcboss2022

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Well all ICE together around 800gr with all recovery stages done. I say this because I separate D and L and I must recrystallize the oil rest of each crystallization adding the dried rest powder of the acetone wash...hard job hahah
 

Bartholomeus

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After using 950ml of pure meth oil, you get 800gr racemic meth is this correct?
When separating D and L isomer, how much D isomer do you get out of it?
 

btcboss2022

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800gr with D and L weight together I don't get racemic one I separate isomers first directly from the oil.
 

Bartholomeus

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Is this also possible? I hear for this for first time - separating isomers directly from the oil
Can you explain what is the process please? How to separate D from L in the oil?
 

btcboss2022

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Of course is possible I told you I did it, unfortunately I can't share that info my partners don't allow me that because we invest some money to obtain that method. Thanks.
 

G.Patton

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It's simple procedure with d-trataric acid. Look at this method, same with meth.
 

situ1984

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Should I use d-tartaric acid directly? Can I get D by cleaning the oil produced by btcboss2022 method?
 

G.Patton

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Can you be more specific? What method do you refer to? What do you mean directly? This method (which I linked) is direct.
 

btcboss2022

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Is not exactly the same is more complex but this method will work too.
 
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