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@William Dampier
Need help with measurements
Instead of using :Valerophenone
I will buy liquid : 2-Bromovalerophenone
If I want to use 1litre
What is the reagents amount I will need per I litrre:
-Hydrobromic acid (HBr) 48%;?
-Hydrogen peroxide (H2O2) 35%;?
-Pyrrolidine (CAS 123-75-1);???
-Ethyl acetate ;???
-Sodium carbonate (Na2CO3) 20% aq solution;???
-Diethyl ether (Et2O) ????
-EtOH 50 ???
-Dibenzoyl-D-tartaric acid ??
-Dichloromethane (CH2Cl2) 830 mL;
-Hexane ????
Hydrochloric acid conc. 35% (HCl);.??
WOULD REALLY HELP IF YOU CAN GET ME MEASUREMENTS FOR USE OF 1 LITRE 2-BROM. PLEASE?????
So that I can cost per reaction, also is the yield estimate about 20% loss
1 litre = 800g a-pvp?
Need help with measurements
Instead of using :Valerophenone
I will buy liquid : 2-Bromovalerophenone
If I want to use 1litre
2-Bromovalerophenone
What is the reagents amount I will need per I litrre:
-Hydrobromic acid (HBr) 48%;?
-Hydrogen peroxide (H2O2) 35%;?
-Pyrrolidine (CAS 123-75-1);???
-Ethyl acetate ;???
-Sodium carbonate (Na2CO3) 20% aq solution;???
-Diethyl ether (Et2O) ????
-EtOH 50 ???
-Dibenzoyl-D-tartaric acid ??
-Dichloromethane (CH2Cl2) 830 mL;
-Hexane ????
Hydrochloric acid conc. 35% (HCl);.??
WOULD REALLY HELP IF YOU CAN GET ME MEASUREMENTS FOR USE OF 1 LITRE 2-BROM. PLEASE?????
So that I can cost per reaction, also is the yield estimate about 20% loss
1 litre = 800g a-pvp?
Marvin "Popcorn" Sutton
Expert
- Joined
- Jul 25, 2021
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