OTC Synthesis of P2P

T0lek511

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Chapter 1 Benzene​


Reagents


  • 100 g Sodium Benzoate 0,877 mol (C7H5NaO2)
  • 60 g NaOH 1,5 mol
Procedure

  • 1. mix it and crush it
  • 2. Carry out a dry distillation of a mixture of benzoate and hydroxide
  • 3. Pre-distill the orange liquid to produce a transparent benzene solution (benzene boils at 353.25K)

Chapter 2 Chloroacetone​

https://www.youtube.com/watch?v=9Lfv3_9xOqo&t=457s&ab_channel=Pavel%C5%A0ejvl

Warning!!! Its tear gas!!!

Reagents


  • Acetone 500ml 6,81 mol
  • Calcium hypochlorite 100g 0,7 mol (Ca(ClO)₂)
  • A few drops of 96% H2SO4 (drain cleaner) as a catalyst
Procedure

  • 1. Combine it
  • 2. Add a few drops of H2SO4 and check pH stop adding drops when the pH is around 4
  • 3. Distill it(acetone boils around 329K opposite chloroacetone boils around 392K and dichloroacetone boils around 446K. You want chloroacetone.)

Chapter 3 P2P​

Reagents

  • Chloroacetone 100ml 1,25 mol
  • Benzene 110ml 1,25 mol (C6H6)
  • AlCl3 10g as a catalyst
Procedure

  • 1. Combine it
  • 2. Distill it
Yield is very low about 5-10%. This is theoretical synthesis I didnt do it.
 

TucoSalamanca.

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how many degrees am i distilling it
Am I distilling at 118 degrees?
 

G.Patton

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TucoSalamanca.

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are these instructions wrong
 

G.Patton

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There is not full information, very poor tutorial.
 
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