- Language
- 🇹🇷
- Joined
- Nov 25, 2024
- Messages
- 22
- Reaction score
- 4
- Points
- 3
Propionyl chloride, benzoyl chloride prepared via propionic acid The 1:1 molar ratio of reactants was chosen.
10 mol propionic acid ≈ 747 mL 10 mol benzoyl chloride ≈ 1161 mL (~1:1 molar ratio) in a 2000 mL flask Vertical distillation through a 200 mm column
45-69'C (most collected above 64-69'C) by evacuating a stream of HCl gas from the reaction while finally heating to 190'C to yield 340 g of distillate.
Yield 340 Gr
Note : Really very dangerous synthesis think twice.
10 mol propionic acid ≈ 747 mL 10 mol benzoyl chloride ≈ 1161 mL (~1:1 molar ratio) in a 2000 mL flask Vertical distillation through a 200 mm column
45-69'C (most collected above 64-69'C) by evacuating a stream of HCl gas from the reaction while finally heating to 190'C to yield 340 g of distillate.
Yield 340 Gr
Note : Really very dangerous synthesis think twice.