N-Ethylpentedron (NEP) Synthese

[chemicals]

Hello, I am planning to synthesize N-ethylpenderone (NEP) in medium scale (5-10kg) as the demand has increased in the recent times for this stuff, if anyone has experience with this synthesis, hit me up maybe I am gonna need help.

As I read it is the same synthesis as APVP, but I have to use ethylamine instead of pyrrolidine.

If anyone tried to make this stuff, please give me some pictures of the procedure, as anything can be helpful at the start. Thanks!

 

[ttotisud]

Good idea, I am also interested in this.

 

[chemicals]

yes I think its not just as, recent times it was a missing item with growing demand

 

[ttotisud]

As I asked some people here are the reagents step by step so far:​

1. 2-bromo valerophenone
2. Ethylamine 70%
3. DCM (Methylene Chloride)
4. MgSO4 (Magnesium Sulfate)
5. NMP (optional for faster and higher yielding)
6. acetone
7. HCL conc. 37% (Hydrochloric Acid 37% Solution)

On quantities, I have to do more research.​

Anyone with more cooking experience than me, do you have some opinions on this recipe? @G.Patton , @Marvin "Popcorn" Sutton or @WillD

 

[OreoBetor]

Easy work thanks

 

[nep consumer113]

is this nep you made and if yes how?

 

[Marvin "Popcorn" Sutton]

Hello, NEP can be done as a-pvp and as 4mmc. We can work together on this. But I don't have any pictures, unfortunately.

 

[ttotisud]

Thanks, we have made 4mmc before successfully, but we can barely find any information and synthesis about NEP. But we will try it until we can make it, and gonna share with you if interested.

 

[Marvin "Popcorn" Sutton]

It's very interesting, write it up. I am always ready to help with advice.

 

[nep consumer113]

Very interesting but not much of a chemist. recomendations for beginners? Also wanna make nep

 

[nep consumer113]

you have to use ethylamine free base sln.

 

[nep consumer113]

http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/nep-synthesis-including-valerophenone-and-nitroethan.6684/

This guy made a post about it

 

[nep consumer113]

I also made note on all the info a could find.
Pm me if u want