6CL-ADB-A (MDMB-5en-HENACA) solid product synthesis

[lutte123]

Anybody can help and share recipe how to prepare this noid?
I tried to follow 5CL recipe both methods - ice water quench or DCM extraction + EtOH crystalisation too but not able to get solid (crystals) product.
Precursor works very good with bromopentene, but with bromohexene always got just oil/sticky paste product.

 

[lutte123]

Brother what are you talking about? Your reply makes no sense for me

 

[sashawhitelabx]

Hello, actually the product seems to be stable oil and not crystal forming. We are trying different route for reCrystallization but think is stay oily.

 

[lutte123]

I saw pictures at chinese ads of 6CL as yellow powder, one NL vendor is selling 6CL as powder too. I did many attempts with different conditions and in each case got oily product only. Maybe what they call 6CL is not an analogue of 5CL with one more CH2 group, could be MDMB-6-chlorohenaca or any related analogue..