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Found this comment below a video about synthesis (Al/Hg2)
"If you dont want to work with toxic Mercury salts, then you can go with a two step synthesis:
Step 1: Fe + HCl reduction of P2NP or with Zink in GAA followed by steam destillation to yield P2P
Step 2: Reductive ammination with NiCl2 dissolved in 20% ammonia and portionwise additon of Zink powder
Its an easy more enviroment friendly and less toxic synthesis"
But no idea how much from which substance should be used for, as example, 250g p2np.
And ideas, thoghts or experiences?
"If you dont want to work with toxic Mercury salts, then you can go with a two step synthesis:
Step 1: Fe + HCl reduction of P2NP or with Zink in GAA followed by steam destillation to yield P2P
Step 2: Reductive ammination with NiCl2 dissolved in 20% ammonia and portionwise additon of Zink powder
Its an easy more enviroment friendly and less toxic synthesis"
But no idea how much from which substance should be used for, as example, 250g p2np.
And ideas, thoghts or experiences?