Help with conversion of BMK powder 718-08-1 to P2P

LordCrackingtonson

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Hello Breaking Bad family...

I have been searching but cannot find any information regarding conversion of BMK powder 718-08-1 to P2P.

Ethyl 3-Oxo-4-phenylbutanoate

Has anyone got further information or had success with conversion?
 

G.Patton

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Hi. I haven't found clear data about this reaction but according first reaction with 74% yield, you can carry out simple acid hydrolysis.
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0oEdP9LiK4
 

btcboss2022

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74% could be the highest yield from BMK powders to P2P nowdays. I will pay attention to this CAS. Thanks.
 

LordCrackingtonson

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Upon further investigation, seems cas 718-08-1 is close derivative of MAPA called EGPA.

Should convert to P2P using the simple acid hydrolosis as posted by Mr Patton.

** interesting pick up about the ester exchange from ethyl to methyl using methanol and then that causing Phenylacetylcarbinol as a by product.

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loadingST

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So did anyone had bought from this new legal BMK alternative, and have worked his way up to amph/meth any new byproducts or problems with synthesis releted to this new oil?Is destilation needed to get enough pure bmk I woud ask experts how much time woud it need under acidic reflux to give P2P ?
 
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