Synthesis MN-001 yield 15 g
Required equipment:
Electric hob with closed burner
Funnel for bulk materials (with a wide bottom)
Flat-bottomed flask 1000 ml
Reverse refrigerator
Large basin with wide sides
Required reagents:
Distilled water
PMN (1-Nafindol) - 15g
Amyl bromide - 18g
TBAB (tetrabutylammonium bromide) - 3.75g alkali - NaOH
Work progress:
1) Take distilled water and dissolve the alkali in a proportion of 0.35-0.45 sodium hydroxide per 0.75 ml. 150-200 ml of water is enough.
2) Add PMN, then mix everything, add amyl, and again, after mixing everything, add TBAB thoroughly.
3) Put on the reverse refrigerator.
4) Mix everything thoroughly and heat at a temperature of 75-85 degrees until smooth.
5) The synthesis takes 12-18 minutes, after which the heating stops, the flask was intensively mixed throughout the entire time.
6) It is important not to miss the moment when bubbles begin to form on the surface of the lower layer, slightly colored transparent - these are polymers.
7) As soon as the polymers are noticed, the synthesis stops, and the reaction mass is merged into a glass.
8) Select the top oily layer in a separate cup.
9) 2-3 times pour boiling water there and rinse to get rid of possible impurities and unreacted products.
10) Then the top layer is collected, poured into a small cup and placed in a dark, ventilated place for 12-18 hours.
11) After 18 hours, everything that has not crystallized is poured out, what has crystallized is washed several times and left to dry.
At the output we get 15 g MN-001
Required equipment:
Electric hob with closed burner
Funnel for bulk materials (with a wide bottom)
Flat-bottomed flask 1000 ml
Reverse refrigerator
Large basin with wide sides
Required reagents:
Distilled water
PMN (1-Nafindol) - 15g
Amyl bromide - 18g
TBAB (tetrabutylammonium bromide) - 3.75g alkali - NaOH
Work progress:
1) Take distilled water and dissolve the alkali in a proportion of 0.35-0.45 sodium hydroxide per 0.75 ml. 150-200 ml of water is enough.
2) Add PMN, then mix everything, add amyl, and again, after mixing everything, add TBAB thoroughly.
3) Put on the reverse refrigerator.
4) Mix everything thoroughly and heat at a temperature of 75-85 degrees until smooth.
5) The synthesis takes 12-18 minutes, after which the heating stops, the flask was intensively mixed throughout the entire time.
6) It is important not to miss the moment when bubbles begin to form on the surface of the lower layer, slightly colored transparent - these are polymers.
7) As soon as the polymers are noticed, the synthesis stops, and the reaction mass is merged into a glass.
8) Select the top oily layer in a separate cup.
9) 2-3 times pour boiling water there and rinse to get rid of possible impurities and unreacted products.
10) Then the top layer is collected, poured into a small cup and placed in a dark, ventilated place for 12-18 hours.
11) After 18 hours, everything that has not crystallized is poured out, what has crystallized is washed several times and left to dry.
At the output we get 15 g MN-001
