I've been doing 3cmc synthesis with both organic and water layer successfully for quite some time now, however I keep having trouble with freebase only. I tried ethyl acetate and dcm with same results. After draining water layer, I add acetone and start acidifying slowly. Rm quickly darkens and black blobs of water from acid appear. I reached ph of 6, stored the freebase in room temperature for a bit of evaporation and the color became yellow again with no precipitation whatsoever. Haven't had any problems with both freebase and water together.. any ideas?
You are using an out of date browser. It may not display this or other websites correctly.
You should upgrade or use an alternative browser.
You should upgrade or use an alternative browser.
3cmc freebase acidification
- Thread starter draconic123
- Start date
- Language
- 🇩🇪
- Joined
- Sep 23, 2022
- Messages
- 158
- Reaction score
- 71
- Points
- 28
Why do you want to do this?
I see no sense in it, you cant evaporate freebase and expect that crystals will form...you can put it into freezer but the results are not the same as with water
I see no sense in it, you cant evaporate freebase and expect that crystals will form...you can put it into freezer but the results are not the same as with water
- Joined
- Jun 2, 2023
- Messages
- 24
- Reaction score
- 6
- Points
- 3
I dont want to get crystals, I want to get powder faster. So I could clean it because crystals all come out dirty anyway.
- Language
- 🇩🇪
- Joined
- Sep 23, 2022
- Messages
- 158
- Reaction score
- 71
- Points
- 28
About Us
Our team brings together the best specialists from different fields.
We are ready to share our experience, discuss difficult issues and find new solutions.