I am not sure if this merits its own thread, but outlined here is a common method for making 2c-b. Starting from the benzaldehyde and utilizing the NaBH4/ CuCl2 reduction+hydrogenation and finally bromination with N-Bromosuccinimide (NBS). A recent methodology with safer procedures and chems...
Okay so I understand that 2c-h freebase is not stable and I am someone who is going through benzo withdrawals and so I will admit there can be some time between doing certain steps….
I have some 2,5-DMOBA and iv been gathering everything I need to turn it into 2c-h and then from there a whole...
stole this from the vespiary, original synth by sonson but i broke it into steps because i dont like reading paragraphs ^^;
1. Into a three-necked 1L round bottomed flask fitted with an argon inlet, a condenser, an additional funnel and a stirring magnet, there was added 20g LAH to 350ml dry...
Well Howdy there folks! There’s a lot of info and conversations and loosely, reliable syntheses on many forums discussing using 2 particular reagents, but I need something objective.
I’m looking for this “gold standard” synth everyone is having success with using Sodium Borohydride and...