4'-methylpropiophenone
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4-MMC (mephedrone) synthesis. Bromination in dichlormethane.
We'll consider mephedrone (4MMC) synthesis in this article. Dichloromethane (DCM) is used as a solvent. It has a low boiling point (~40 °C) and synthesis procedures take a little time. Work conditions: Air temperature 20-24 ºC; Relative humidity <60%; Well-ventilated room (with air...- Marvin "Popcorn" Sutton
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- 4'-methylpropiophenone 4-methylephedrone 4-methylmethcathinone 4-mmc cas 1189726-22-4 cas 5337-93-9 instruction m-cat mephedrone synthesis tutorial
- Replies: 120
- Forum: Methcathinones
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4'-Methylpropiophenone iodination to 2-iodo-4'-methylpropiophenone by iodine/cooper(II) oxide. Video manual.
Reaction scheme: Reagents: 4'-Methylpropiophenone (cas 5337-93-9) 5 kg; Сooper(II) oxide (CuO) 2.7 kg; Isopropyl alcohol (IPA) 50 l; Iodine 6.5 kg; Equipment and glassware: 100 L Batch reactor, which is equipped with drip funnel, top stirrer, thermometer, temperature control system...- WillD
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- 2-iodo-4'-methylpropiophenone 2-iodo-4'-methylpropiophenone synthesis 4'-methylpropiophenone 4-mmc synthesis cas 1189726-22-4 cas 236117-38-7 cas 5337-93-9 cathinone mephedrone synthesis video manual
- Replies: 27
- Forum: Methcathinones
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2-Bromo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone. Bromination in DCM or GAA.
Reaction scheme: Reagents: 4-methylpropiophenone (cas 5337-93-9) - 1000 g; Dichloromethane (DCM) or glacial acetic acid (GAA) - 3000 ml; Bromine (Br2) - 1080g, 348 ml; Sodium bicarbonae (NaHCO3) solution; Distilled water; Magnesium sulphate (MgSO4); Equipment and glassware: Three necked...- WillD
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- 2-bromo-4'-methylpropiophenone 4'-methylpropiophenone 4-mmc cas 1451-82-7 cas 5337-93-9 cathinone mephedrone
- Replies: 17
- Forum: Methcathinones
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Mephedrone (4-MMC) synthesis from haloketone in ethyl acetate. 1-10 kg Scale.
Reaction scheme: Reagents: 1. 4'-Methylpropiophenone (cas 5337-93-9) 1 kg; 2. Hydrobromic acid 48% 1300 ml; 3. Hydrogen peroxide 35% 750 ml; 4. Sodium/potassium hydroxide 25% (NaOH/KOH) aqueous solution; 5. Distilled water; 6. Ethyl acetate 6 l; 7. Methylamine 40% aq - 2 l; 8. Acetone - 8 l...- WillD
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- 2-bromo-4'-methylpropiophenone 4'-methylpropiophenone 4-mmc ethyl acetate 4-mmc synthesis cas 1189726-22-4 cas 1451-82-7 cas 74-89-5 mephedrone ethyl acetate synthesis mephedrone synthesis methylamine
- Replies: 60
- Forum: Methcathinones