You can scale it proportionally (in large amounts methylamine may be added in more parts)
Reagents:
1. 2b4m 100g;
2. Ethyl Acetate 500ml;
3. Distilled water ~2l;
4. NaOH 100g;
5. Methylamine HCL 150g;
6. Acetone 500-1000ml.
Equipment:
1. Magnetic stirrer;
2. Beaker 200ml (can be any volume)...
Whats this look like to you? I did a couple things. I heated ammonium chloride and formaldehyde with an alihn condenser and 110° turndown vacuum fitting on top and vacuum pump for a few hours and let it cool and filtered it. Then I distilled the liquid under vacuum for a couple hours and...