cas 109555-87-5

Reaction scheme: Equipment and glassware: 50 L Batch reactor, which is equipped with drip funnel, top stirrer, thermometer, temperature control system (cooling) and reflux condenser; 10 L Flask; Retort stand and clamp for securing apparatus (optional); Reflux condenser; Top stirrer; Heating...

Reagents: Indole (cas 120-72-9) 1000 g; Dichloromethane (CH2Cl2) 15 l; Tin(IV) chloride (SnCl4) 2000 ml; 1-Naphthoyl chloride (cas 879-18-5) 1627 g; Nitromethane (cas 75-52-5) 10 l; Distilled water 20 l; Ethyl acetate (EtOAc) 15 l; Sodium or magnesium sulphate (Na2SO4 or MgSO4); Equipment and...