cas 705-60-2

Benzaldehyde and nitroethane Henry condensation. https://bbgate.com/threads/1-phenyl-2-nitropropene-p2np-video-synthesis-from-benzaldehyde-and-nitroethane-henry-reaction.52/

479Mb (.mp4) 1-Phenyl-2-nitropropene (P2NP) reduction to α-methylphenylethylamine by aluminium amalgam. https://bbgate.com/threads/amphetamine-synthesis-from-p2np-via-al-hg-video.196/

https://bbgate.com/threads/synthesis-of-amphetamine-from-p2np-via-al-hg-video.196/

Reagents: 1-Phenyl-2-nitropropene (P2NP; cas 705-60-2) 1000 g; Methanol (MeOH) 10 L; Sodium borohydride (NaBH4) 470 g; Hydrogen peroxide (H2O2) 30% 6 L; Potassium carbonate (K2CO3) 1800 g; Hydrochloric acid (HCl) 37% aq; Dichloromethane (CH2CI2) 5 L; Sodium hydroxide (NaOH) 5 L 25% aq...

Reaction scheme: Equipment and glassware: 50 L batch reactor with a reflux condenser, top stirrer and heating apparatus in a set-up; Drip funnel; Conventional funnel; Laboratory grade thermometer (up to 150 °С); Several buckets for 10 and 20 L; Measuring cylinder for 1 L; Vacuum source...

Reaction scheme: Equipment and glassware: 10 L Flask; Retort stand and clamp for securing apparatus (optional); Reflux condenser; Funnel; Vacuum source; Laboratory scale (0.1-500 g is suitable) - optional; Measuring cylinders 1000 mL and 100 mL; Water bath; Glass rod and spatula; Filter...

Reagents: 1-Phenyl-2-nitropropene (P2NP; cas 705-60-2) 1.63 g, 10 mmol; Powdered iron (Fe) 3 g; FeCl3 0.6 g; Hydrochloric acid (HCl 36% aq.) conc. 4 ml; Toluene 15 ml; Water 55 ml; Hydrochloric acid 3N (10.45%) HCl 25 ml; Sodium bicarbonate (NaHCO3); Magnesium sulfate (MgSO4); Equipment and...

Reagents: Lithium aluminum hydride (LAH; cas 16853-85-3) 12 g; 1,4-Dioxane 300 ml; 1-Phenyl-2-nitropropene (P2NP; cas 705-60-2) 10 g; Sodium hydroxide (25% NaOH) aq. solution; Acetone ~50 ml; Sulfuric acid ~10 ml; Equipment and glassware: Two-naked round bottom flask 1 L; Retort stand and...