Starting reagents and materials
6 g Synthetic ephedrine hydrochloride racemate
1.8 g Red phosphorous (P)
12 g Iodine (I2)
100-150 ml H2O
3 g Sodium thiosulfate (Na2S2O3)
24 ml 25% NaOH
250-300 ml DCM
100 ml Petroleum ether
HCl gas
100 g NH4Cl
25 ml H2SO4 83%
Flasks 250 and 500 ml
Beakers...