Starting reagents and materials
100 ml H2O
7.21 g THF
15.1 g KBrO3
13.6 g KHSO4
14 g Na2S2O5 dissolved in 150 ml H2O
150 ml H2O
250-300 ml DCM
50 g Na2SO4
3.38 g NaHCO3 dissolved in 15 ml H2O
3-neck flask 1000 ml
Thermometer
High efficiency double circuit reflux
Magnetic stirrer
Cold...