indole
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TMCP-indole synthesis (UR-144 intermediate, cas 895152-66-6). Large scale.
Reaction scheme: Equipment and glassware: 50 L Batch reactor, which is equipped with drip funnel, top stirrer, thermometer, temperature control system (cooling) and reflux condenser; Funnel; Several buckets 10 and 20 L; Vacuum source; Laboratory scale (1-2000 g is suitable); Measuring cylinder...- WillD
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- a-834735 cannabinoid synthesis cas 24303-61-5 cas 895152-66-6 indole tmcp-indole synthesis ur-144 xlr-11
- Replies: 15
- Forum: Cannabinoids
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3-(1-Naphthoyl)indole Synthesis
Reagents: Indole (cas 120-72-9) 1000 g; Dichloromethane (CH2Cl2) 15 l; Tin(IV) chloride (SnCl4) 2000 ml; 1-Naphthoyl chloride (cas 879-18-5) 1627 g; Nitromethane (cas 75-52-5) 10 l; Distilled water 20 l; Ethyl acetate (EtOAc) 15 l; Sodium or magnesium sulphate (Na2SO4 or MgSO4); Equipment and...- WillD
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- 1-naphthoyl chloride 3-(1-naphthoyl)indole synthesis cas 109555-87-5 cas 879-18-5 indole jwh 018 jwh-018
- Replies: 34
- Forum: Cannabinoids