indole

  1. WillD

    TMCP-indole synthesis (UR-144 intermediate, cas 895152-66-6). Large scale.

    Reaction scheme: Equipment and glassware: 50 L Batch reactor, which is equipped with drip funnel, top stirrer, thermometer, temperature control system (cooling) and reflux condenser; Funnel; Several buckets 10 and 20 L; Vacuum source; Laboratory scale (1-2000 g is suitable); Measuring cylinder...
  2. WillD

    3-(1-Naphthoyl)indole Synthesis

    Reagents: Indole (cas 120-72-9) 1000 g; Dichloromethane (CH2Cl2) 15 l; Tin(IV) chloride (SnCl4) 2000 ml; 1-Naphthoyl chloride (cas 879-18-5) 1627 g; Nitromethane (cas 75-52-5) 10 l; Distilled water 20 l; Ethyl acetate (EtOAc) 15 l; Sodium or magnesium sulphate (Na2SO4 or MgSO4); Equipment and...
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