mescaline synthesis
-
P
Synthesis notes of Mescaline from 3,4,5-TMBA I update real time as I make a progress
Here I'll document my Mescaline synthesis from 3,4,5-trimethoxybenzaldehyde then after I optimize the reaction I'll write the documents. My goal is to achieve good yield using minimum catalyst and nitromethane. 3,4,5-trimethoxybenzaldehyde in a bag Experiment 1: 10g of...- Palocn
- Thread
- 2-heaa mescaline mescaline synthesis nabh4/cucl2
- Replies: 2
- Forum: Amphetamines (Phenylethylamines)
-
D
Mescaline synthesis mishaps
QuestionI have tried to synthesize mescaline from 3,4,5-trimethoxybenzaldehyde via two different routes. Everything seemed to work well until the last step, yet no desired product was obtained. Does anyone have an idea of what might have gone wrong? My route was in principle the following: 1)...- David Darling
- Thread
- mescaline synthesis
- Replies: 5
- Forum: Question-Answer
-
Mescaline Synthesis With Nitromethane. 1000g Scale.
Reagents: 3,4,5-Trimethoxybenzaldehyde (cas 86-81-7) 1000 g; Acetic acid 5 L; Nitromethane (cas 75-52-5) 2 L; Cyclohexylamine (cas 108-91-8) 100 ml; Distilled water ~17 L; Isopropyl alcohol (IPA) ~23 L; Sodium borohydride (NaBH4) 1200 g; Copper chloride (CuCl2) 72 g; Sodium hydroxide (NaOH) 25%...- William D.
- Thread
- cas 6316-70-7 cas 642-73-9 cas 832-92-8 cas 86-81-7 mescaline mescaline synthesis nitromethane peyote tmpea trimethoxybenzaldehyde
- Replies: 71
- Forum: Amphetamines (Phenylethylamines)