methylamine hcl synthesis

Whats this look like to you? I did a couple things. I heated ammonium chloride and formaldehyde with an alihn condenser and 110° turndown vacuum fitting on top and vacuum pump for a few hours and let it cool and filtered it. Then I distilled the liquid under vacuum for a couple hours and...

I would just like to know whats the best way to get formaldehyde for a small-scale synthesis. Since formaldehyde is very regulated in EU I have also thought about synthesizing it myself with methanol but since the temperature and equipment needed are insane I just want to buy some on the low...

Just wondering what is the best way to purify methylamine created by reacting formaldehyde and ammonium chloride (which is at the end the only contaminate after dichloromethane and methanol wash). What I found was that the solubility in ethanol(pure) for methylamine is 29.1g/100g(at 78*C) and...

I am done with doing a formaldehyde and ammonium chloride synthesis of methylamine it's too dirty and dealing with ammonium chloride is hell. Does anyone have any experience successfully doing a fe/hcl reduction of nitromethane to the HCL salt? or something similar. It seems like an easy way to...

https://bbgate.com/threads/methylamine-hydrochloride-synthesis-large-scale.617/ NileRed video https://www.youtube.com/watch?v=wuyouolU5LY