Synthesis of A Sulphate via Oxime Reduction (Report 2)
Previously, a synthesis via aluminum amalgam was carried out with a low yield of the target amine
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The...
Reactions proceed according to Scheme 1
Reagents and Materials:
8.1 g of aluminum
0.05 g of mercury(II) chloride
5 g P2P
2 g of hydroxylamine or a mixture (50-60 ml of IPA (or ethanol) + 2.5 g of NaOH + 4.55 g of hydroxylamine hydrochloride)
50 ml of ethanol
2-liter flask
2 liters of ice-cold...