Help God! My D-Meth is going weird!!

[qwe111]

I passed hydrogen chloride gas through a mixture of D-meth and acetone and got a shiny powder.
It is different from the hydrochloride powder. It is like very fine "ice"!
I want to get the hydrochloride of meth, then dissolve the hydrochloride and recrystallize to get large crystals!
But I don't know what I did wrong?
Now can I dissolve this fine ice in water and recrystallize it?
Or do I have to dissolve it and add sodium hydroxide to get FB oil, and then do it again?
Oh God, someone please tell me what to do!!!

 

[WillD]

Can you show a photo of the product and reveal the method of synthesis? The forum has published crystallization methods in different solvents, including water crystallization. But it is better to first get a powder to recrystallize this.

 

[qwe111]

Hi Sir, I just want to know if "ICE" can be directly dissolved and recrystallized with solvent?
Or do I have to use alkali to extract the oil? Then do hydrogen chloride gas to get methamphetamine hydrochloride, and then crystallize it into large crystals?

 

[qwe111]

Hi gentlemen, I did the same method twice and got different results!
The first one on the left is the hydrochloride, I know it can be dissolved in a certain proportion of solvent and recrystallized!
The second one is the same method, it is more like a crystal!
I want to know if the second one can be dissolved in a solvent, and then evaporate the solvent to get large crystals???

 

[qwe111]

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[G.Patton]

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Methamphetamine Recrystallization

• Novator
• May 27, 2024
• 26
• methamphetamine recrystallization

d,l-Methamphetamine Recrystallization...