How to completely remove dcm without rotary evaporator?

qwe111

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When I removed DCM, I found that the mixture was still boiling even though the temperature had reached above 100. But nothing is condensing in the condenser. Does this mean there is still DCM in the mixture that has not evaporated? I don't have a rotary evaporator. What should I do to completely remove DCM? Do you need to stir? Or vacuum distillation?
 

hacke8

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After DCM extraction and drying, DCM can be removed by distillation at 90-110 degrees.
 
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