Mephedrone (4-MMC) Synthesis [2B4M, Etyhyl Acetate, Methylamine HCl]

c01db100d

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Can we replace

MA HCI to
METHYLAMINE (mono) 40%
CAS.No: 74-89-5

Ordered

2-Bromo-4-methylpropiophenone 1451-82-7
Acetate
NaOH
Acetone


Tell me if we need something more ?
 

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Yes u can and dont need anything more
 
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c01db100d

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@$!$ , @MMX .
After we got delivery
And after setup equipment
Guide me for synthesis process
And the quantity ratio for synthesis.
 

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Ask mmx i no take time.All u have on bbgate
 

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But i can say normal dont need any lab equipment this all way 0 if u are Smart on big or small scale can made without lab equipment
 

Dr. MMX

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yes u can use 40% 200 ml aq,but probably you will have less yield, usually its not the best quality of 40% aq, hjard to get good
 

Osmosis Vanderwaal

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🤔 so some jack leg home chemist 8s makining Methylazanium chloride, and cleaning it so well that after the person released the methylamine IT IS GOING TO BE MORE PURE THAN THE SIGMA ALDRIDGE 40% METHALAMINE SOLUTION?! Pardon me, I've done an ounce of cocaine since Friday, but I find that very fucking hard to believe. I've, ade it a few times made chloroform and distilled methanol t9 clean ot up and it was no where near even 90% purit u
 

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Can you describe your point in different words? I am not sure if I didnt catch irony there :)
 

Dr. MMX

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hcl acid, i didnt note it in reagents, my mistaker
hcl acid is needed as well
 
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Dr. MMX

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i believe you should describe it yourself, becasue if you did exactly the same, the result would be the same as well so you had to misssomething. Check it again
 

c01db100d

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I type in pm ,what i do. Give 5 min
 

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Dolar is speaking truth. you just start by reading all the posts in methcathynones, watch videos and you know all
 
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hacke8

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It's a very worthwhile line to buy. Thank you for your selfless dedication. Sir, there are two small questions. Between steps 3-7, how many degrees Celsius should the temperature be controlled below?
 

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below 55-60
just use water bath so you dont need to check it really
when i didnt ujse water bath, i spend like 15 mins to wait to add it in 3 parts :) and you never know how much it will heat.
 

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I mean sorry *
always check :) but dont mind about it :)
 
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hacke8

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Thank you for your reply. More detailed content can help you better complete the experiment.
 

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I believe temp there doesnt matter as long its not over 55-60. Future tests will be focused on adding different % acetone of remaining freebase before acifification :)
 

hacke8

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Sir, I sent you a private message. I need your help.
 

TucoSalamanca.

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metilamini eklerken kaç dereceyi geçmemeli
 

TucoSalamanca.

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ve eklerken soğuk su banyosu mu yoksa sıcak mı
 

Dr. MMX

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Please use english, so others may understand as well.
max 55-60 degrees
its cold bath, water from fridge is ok
remmeber to not put bath before bk4 is disolved in EA becase it may cool down to not let it dissolve if its not crushed well
 

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My methyloamine hcl looks like it
 

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Dr. MMX

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structure is similar, but not sure aboutg color, but its photo etc
ii think it sjust difference a size of crystals, but never know what it is
 
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I try change naoh because is 96% pure
I will buy pure and then see
 

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i got pure
 

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Maybe there is problem
 

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maybe it wasnt properly storaged (ma) maybe recrystalize it and see the output if it will look like on photo i attached
 
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