Tread ? i just want some advice tips... CAS bmk powder outside

[Botsauto-Dutchland]

So after some strugles we start with nothing

cas 5449-12-7 Conversion Yields phosforic acid 75/85 or sulfuric acid 98..

I will do this outside i have 1kg bmk glycidate sodium salt.

any tips i not yet own any type of glasware exept some adapters and a lift..

in the time i dont stir or my accu is stirring i will add formic acid to nh4carbonate... or is there a faster better way to get formamide ?? i just heat the solution to 160c for an hour.. vacuum distilation is not possible now.

its sounds or looks like i am lazy but i cant do some test i will do it in 3 steps 1kg bmk powder -->p2p next night steam distil and preparing formamide, step 3 leuckart

any tips are very welcome
use stainless steel pot ?
hdpe for the first conversion p2p refluX needed in meaning of yield or just add acid.
glass will be arived at leackart step.

thanks for all advice

ps i hate this way working with chemicals normally i realy enjoy just watching the reaction and take your time.. but now i cant and have no experiance like this style

 

[Brain]

Great reasoning!
But all problems concerning synthesis are better discussed here - b/amphetamines-phenylethylamines.2/

 

[Botsauto-Dutchland]

Anyway i tried but its not a link if it suposed to i dont know.. my excuses

ps somebody experiance with sodium lime and the carboxilic acid sodium salt reaction..
so i add my cas 5449-12-7 to lime powder( Soda lime is a mixture of NaOH and CaO)
Tell me how i move it to right location

 

[Brain]

If you can't open the link, go to "synthesis technologies and analysis"

 

[Brain]

Was it successful, bro?

 

[Botsauto-Dutchland]

i found it ! wasnt here for a wile litle bit lost

 

[StarWars]

Why u buy powder bmk glicydate if is Simple made speed from p2np and also is Simple made p2np ??

 

[Brain]

Great!
But if you have any additional questions, be sure to ask!

 

[Botsauto-Dutchland]

wy its cheaper ??? p2np cost you 300/kg the bmk powder 150/ kg and i hate the iron mess. and i dont have Nabh4 than its a great precursor

 

[UsernameRequired]

If i’m not mistaking the yield is better with P2NP —> P2P and you can try to make P2NP with Benzaldehyde. The forum posted a detailed video on how to make it. Benzaldehyde in general is very cheap ( I can get it myself for around 40$/kg )

 

[Botsauto-Dutchland]

yes or you can make it from toluene but the nitroethane ? aldol reaction i tried it once but i did something wrom and getting nitroethane is not so easy ?

 

[Botsauto-Dutchland]

to make p2np i need nitroethane its also expensive, its not worth it for me the
glycidate is cheap and only acid needed to convert and the ammonium formate/formamide is also cheap and easy to get those chemicals.