Syntéza glycidátu BMK (sodná sůl) z benzaldehydu

Arakava

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I added NAOH and stirred for 12 hrs at RT and 2 hrs at 60°c and let it cooled down. But it's still liquid. I think there is too much water in it. What should I do? Should I add hcl or first separate layers with toluene? Tnx
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realboss

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If I replace Benzaldehyde with piperonal same amount end product is pmk ?
Is everything same every step just replace piperonal with Benzaldehyde
@G.Patton plz help boss 👆
 

G.Patton

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Hello, probably yes. We haven't carried out an experiment.
 
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