BMK glycidate (sodium salt) synthesis from benzaldehyde

haze2000

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Jungle method ( HDPE Barrels) wont work with this procedure because of water traces?
 

G.Patton

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Probably yes. I'm not sure about what condition are you talking about.
 

G.Patton

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What? What do u mean? HDPE is plastic. How it can be hygroscopic?
 

jasper

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Is their any substitute? Of Methyl 2-chloropropionate?
 

virus0815

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can Methyl 2-chloropropionate be replaced?
 

G.Patton

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Yes, by ethyl 2-chloropropionate, but this reaction is longer.
 

virus0815

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hey,thanks a lot for the answer.
even though the reaction with ethyl 2-chloropropionate takes longer,at least ethyl 2-chloropropionate can be obtained on the bbgate forum,so thats the one i am going to use
how much ethyl 2-chloropropionate should i use? also 350 g?how much longer would the reaction approximately take?
 
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G.Patton

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hi, same molar equivalent.
Just use exactly EtONa on this stage. Other is the same.
8. When RM is cooled down to 0°С inside the reactor, dry sodium ethylate 200 g (EtONa) addition is started.
 

haze2000

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Can HDPE Barrel (200L) be used for this reaction?
 
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