No, you have to make free base only.
Last edited:
Methamphetamine synthesis from P2P by NaBH4 reduction. Medium-Scale.
- Thread starter G.Patton
- Start date
Hello,
After many tests using Methylamine HCL based on this method I will share the best way that I found to obtain Methamphetamine freebase in big scale:
- Fill the reactor with the 14 L of Methanol
- With stirring dissolve the Methylamine HCL
- Put the reactor temp at 0C(not the mixture temp) and add the NaOH, the temp will increase
- Once the temp come back to 20C add the P2P, the temp will increase stir it during 45min-1 hour
- Add 252gr of anhydrous sodium sulfate
- When the mixture temp arrives to 8C start adding portionwise the NaBH4 not exceeding the 20C
- Once all the NaBH4 has been added let it mixing under 20C during aprox 2 hours until the mixture stops bubbling
- Add the water and continue mixing during 5 min
- Add the DCM and mix it during 10 min
- Stop stirring and let layers get separated
- Keep the bottom layer and discard the upper one( not profitable to extract this aqueous phase)
- Add 200gr of anhydrous sodium sulfate to the saved layer and mix it
- Filter it in Buchner Funnel
- Evaporate the DCM
- Clean and smelly Methamphetamine freebase obtained
;-)
After many tests using Methylamine HCL based on this method I will share the best way that I found to obtain Methamphetamine freebase in big scale:
- 966 gr P2P
- 14 liters Methanol
- 1183 gr Methylamine HCL
- 638gr NaOH
- 452 gr Anhydrous Sodium Sulfate
- 105 gr NaBH4
- 35 L distilled water
- 7 Liters DCM
- Fill the reactor with the 14 L of Methanol
- With stirring dissolve the Methylamine HCL
- Put the reactor temp at 0C(not the mixture temp) and add the NaOH, the temp will increase
- Once the temp come back to 20C add the P2P, the temp will increase stir it during 45min-1 hour
- Add 252gr of anhydrous sodium sulfate
- When the mixture temp arrives to 8C start adding portionwise the NaBH4 not exceeding the 20C
- Once all the NaBH4 has been added let it mixing under 20C during aprox 2 hours until the mixture stops bubbling
- Add the water and continue mixing during 5 min
- Add the DCM and mix it during 10 min
- Stop stirring and let layers get separated
- Keep the bottom layer and discard the upper one( not profitable to extract this aqueous phase)
- Add 200gr of anhydrous sodium sulfate to the saved layer and mix it
- Filter it in Buchner Funnel
- Evaporate the DCM
- Clean and smelly Methamphetamine freebase obtained
;-)
↑View previous replies…
- By btcboss2022
Im trying to improve process yield I will update you tomorrow of how it worked or if its a shit hahahah
- By hunter12
Has anyone tried this route using MgSO4 to dry instead of sodium sulfate? since i ended up with a milky and strong smell solution (from the mixture of MgSO4 and sodium hydroxide) where the water solution would not separated from the meth oil freebase. Tried to to add more and more water and dcm but there was no difference. the whole solution turns into a white precipitate and never separate. i only see small traces of the oil in the solution.
I know your not suppose to do this bit I have added more methylamine hcl and lye then used mgso4 then I quickly vacuum filter the the solution and then quickly poured it back into a fresh clean 10l rbf that i did the synth then added the p2p and nabh4 and it worked no dramas
- By Xiao hua
How to make ice rock crystal ? Can you make a video.
↑View previous replies…
- By btcboss2022
All details about it are posted in many posts you only need to search them, there is a searcher in the forum easy ;-)
Im.gking to be quiet honest and Frank here have any if you tried the product this makes strength wise iits fucken shit yrs you make a product but it does nothing not only me 4 other people said the same thing after producing product for the last 20 years I'm going to tell you all straight unless your reaction has a metal in it don't bother it's the metals that what give the product it's strength leg lithium bitch iodine hypophos/rp p2p aluminium amalgam your reaction has to be one of these else your just waisting time effort and money on producing shit
I'm not having a go at any one I'm just stating the facts thanks to btc bioss keep up the good work I'm going to try and find another method of yours that has metal in so I don't throw this p2p down the toilet all these methods without metal in them are to ifucken.us3l3ss
I'm not having a go at any one I'm just stating the facts thanks to btc bioss keep up the good work I'm going to try and find another method of yours that has metal in so I don't throw this p2p down the toilet all these methods without metal in them are to ifucken.us3l3ss
↑View previous replies…
- By btcboss2022
You can do exactly the same process replacing NaBH4 by an aluminum amalgam as reductor but the rest the same.
Dear sir, can you make a teaching video!？？please！
What can be used instead of sodium borohydride sir！
There are so many methamphetamine recipes, which one is the best?