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This reaction is very good on a small scale
In a large reaction, trying to control the exotherm and the large amount of foam by putting the CuCl2 solution slowly into the flask will not give a high yield, there may be nothing but nitroalkanes and the concentration of nanoparticles will be too small to reduce the nitro, the largest flask possible should be used and the entire CuCl2 solution should be added at once
In a large reaction, trying to control the exotherm and the large amount of foam by putting the CuCl2 solution slowly into the flask will not give a high yield, there may be nothing but nitroalkanes and the concentration of nanoparticles will be too small to reduce the nitro, the largest flask possible should be used and the entire CuCl2 solution should be added at once
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- Jan 11, 2023
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- By RickyKasso
-
06 Apr
What do you consider as "small scale"? Is there any specific amount of P2NP and respective amounts of the other chemicals to have the most optimal and easy going reaction?
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