WillD
Expert
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The reaction with sodium borohydride may get out of control if you do not monitor the temperature. In addition, small-dispersed copper compounds can interfere with the purification of the final product.
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- Oct 19, 2023
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If
the reaction of the sodium borohydride does go out of control, what can I do about it, is the synthesis botched? If there are small dispersed copper compounds, is it impossible for me to remove them when purifying?
the reaction of the sodium borohydride does go out of control, what can I do about it, is the synthesis botched? If there are small dispersed copper compounds, is it impossible for me to remove them when purifying?
- Joined
- May 27, 2023
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I had p2np flare up after an unintentional quick addition with the nabh4 it didn’t do anything negative to my final product.
I filter all the copper compounds out with 2-3 coffee filters after letting it sit after the 80c heating.
I filter all the copper compounds out with 2-3 coffee filters after letting it sit after the 80c heating.