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Could you tell what laboratory equipment is required for the chemical synthesis of 2-CB?
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- By w2x3f5
it all depends on the way of synthesis. you need a starting point and the path you want to follow.
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Henry reaction, flask, reflux condenser, heated magnetic stirrer, water bath (or do it in the microwave), measuring cylinder, vacuum filter Buchner funnel and Bünsen flask and the filters themselves, heat-resistant beakers low spout
Reduction on lithium aluminum hydride is all the same, only ice and a dropping funnel will be needed to drop the styrene solution, and then we drop in ethyl acetate or ethyl alcohol in order to use up the excess lithium aluminum hydride.
Bromination is the same
scales and the like.
Reduction on lithium aluminum hydride is all the same, only ice and a dropping funnel will be needed to drop the styrene solution, and then we drop in ethyl acetate or ethyl alcohol in order to use up the excess lithium aluminum hydride.
Bromination is the same
scales and the like.
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So it would be better to use a chemical reactor to prevent it from exploding and harming me? And if so, what capacity should the chemical reactor be?
Have you made 2C-B before?
thanks!
Have you made 2C-B before?
thanks!
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how will the reactor help you? work correctly with lithium aluminum hydride, everything is as dry as possible, good cooling, the absence of peroxide impurities in the solvent.
I did it in an ordinary three-necked flask in an ice bath, sometimes with explosions and fires, in the first syntheses, then I learned =)
I did it in an ordinary three-necked flask in an ice bath, sometimes with explosions and fires, in the first syntheses, then I learned =)
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It would be better to just not use THF if youre asking questions like this
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mate, I have no idea about chemistry, I'm trying to learn, but it's frustrating, too much information, I still don't know which chemical synthesis to stay with and focus on it, I'm thinking either 2-CB or MDMA, unless I changed my mind, at first I wanted to do the synthesis of LSD but I have seen that the synthesis for the manufacture of only lysergic acid, the precursor of LSD, is very complex and requires many reagents and chemical reactions.
thank you!
thank you!
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My friend, from where did you bought (CAS: 93-02-7)?
And what´s the difference between that and this 2,5-dimethoxy-beta-nitrostyrene?
Thank you! and sorry, but i have no idea about chemistry.
2,5-Dimethoxybenzaldehyde
I found a seller on alibaba that supposedly sells it, but how can I make sure that is that substance when I receive it?And what´s the difference between that and this 2,5-dimethoxy-beta-nitrostyrene?
Thank you! and sorry, but i have no idea about chemistry.
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180 euros for 100g of the styrene and 120 euros for 100g of the aldehyde
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