- Joined
- Jul 11, 2022
- Messages
- 86
- Reaction score
- 42
- Points
- 18
134g/m p2p 45g/m forma so i calculated :100
1,34g 0,5g X22
I have 30 g p2p so X 22 and i got
30g p2p forma 11gx 5 i read the reaction ratio was best 1:5 and formic acid as catalyst
and next i use hcl to Hydrolise but i had just 50% yield but i had to much water in the ammonium formate /formamide i had produced.
now i heated the solution format/formamide to 175 so i hope this helps..
So what is the yield of this method ?
1,34g 0,5g X22
I have 30 g p2p so X 22 and i got
30g p2p forma 11gx 5 i read the reaction ratio was best 1:5 and formic acid as catalyst
and next i use hcl to Hydrolise but i had just 50% yield but i had to much water in the ammonium formate /formamide i had produced.
now i heated the solution format/formamide to 175 so i hope this helps..
So what is the yield of this method ?
- Joined
- Jul 11, 2022
- Messages
- 86
- Reaction score
- 42
- Points
- 18
yield is higher make sure the p2p is purified and dried, if you mix the formamide and p2p it should mix no layers. and preparing formamide/formate heat it up to 180 Short and then lower it until 170 until no water/acid distils and the just wait a bit more. when stop heating put a cap on the glasware so its air tight.
this way i had from p2p oil to a- 100ml to around 70ml but after vacuum distilling so i wasted some a in the pump and in the start and end i had 60ml perfectly clear a oil.
i wish i could write how much powder i could get 10ml a to aphosfate and to sulfate.
if perfectly pure 10ml 9.4g d/l Amphetamine base is mixed with acid(sulfuric98) what should the powder has in weight, and what should be the excact weight in acid to reach ph?
now with not self made oil it is 1ml acid on 10 grams A oil 10 grams powder. reaction is smoking more when no alcohol used for mixing.
should it be cleaner without ether-acid base wash and perform a steam distil from a stainless steal container steamed true a cooler. ( if the oil contains no p2p) what impurity comes with it.
this way i had from p2p oil to a- 100ml to around 70ml but after vacuum distilling so i wasted some a in the pump and in the start and end i had 60ml perfectly clear a oil.
i wish i could write how much powder i could get 10ml a to aphosfate and to sulfate.
if perfectly pure 10ml 9.4g d/l Amphetamine base is mixed with acid(sulfuric98) what should the powder has in weight, and what should be the excact weight in acid to reach ph?
now with not self made oil it is 1ml acid on 10 grams A oil 10 grams powder. reaction is smoking more when no alcohol used for mixing.
should it be cleaner without ether-acid base wash and perform a steam distil from a stainless steal container steamed true a cooler. ( if the oil contains no p2p) what impurity comes with it.