Need help convert bmk 5449-12-7 to free base A-oil

[Saul]

I had already found this out myself because hydrochloric acid has a much too low boiling point. formic acid also has a boiling temperature that is too low.
for this cas we need minimum 140°c so then we need phosphoric acid boiling point 150°c

this is what i meant by wrong methods and they are still online here.

 

[badbreak2]

Its not needed boilingpoint 150 if you make big production just cook till its 120°c and count 6 hours Only what is important you use for 1 kg 5449-12-7 1.5L phosphoric acid 85% and 0.5 L water for each kg

 

[sponsor]

Can someone with know please explane this last step because there are no answers to find.@HEISENBERG

 

[edy's]

Read the whole script of tolmy.its pretty clear i thought.nice one u find

 

[h20]

you also have no clue idiot !
otherwise you didn't ask where you can buy ammonium carbonate

 

[edy's]

Bakery supply store .caled bakers ammonium

 

[Saul]

@oscar412 the last step is not working for me

 

[Davidrobinson]

Whay did you get 75% yield om then

 

[Davidrobinson]

I see. So he cannot get the hydrolsis to work. Just add naoh and water heat at 110 for 2 hours then extract woth dcm when it has cooled T0R

 

[Botsauto-Dutchland]

someone know something about the reaction cas 5449-12-7 with Sodium lime ? Heating together the powders.....

The main components of soda lime are

• Calcium oxide, CaO (about 75%)
• Water, H2O (about 20%)
• Sodium hydroxide, NaOH (about 3%)
• Potassium hydroxide, KOH (about 0.1%).

Or is this a stupid thought ?

 

[Botsauto-Dutchland]

and yield with H2SO4 96% around 65% and h20 it should boil around the 150 otherwise i can add more 96.

 

[Saul]

@ChingShih any updates my friend ?

 

[Botsauto-Dutchland]

No some money problems i have everything prepared for now formamide i could start but i first need 1 more lab stand and a ks 35 balljoint to a female ns 29 hard to find. i printed one but i dont know i dont want to end up @ swim with melting resin and all the smell so i did not do the conversion. and then the steam distil i only have 2 1 necks flask so first i need to fix more glass and then i post results !!

 

[Botsauto-Dutchland]

maybe i go oldschool with rubber and tubes not sure yet but end of the week i want to complete the first full 3L flask i could or i think i cant get 1 kg into the flask with the acid and h2o

 

[Saul]

anyone booking progress here ?

 

[Botsauto-Dutchland]

no running with cocaine, i will progress when its safe

 

[Saul]

How is it possible that when I extract my final liquid with DCM I dont see two layers but just one ?

 

[Sjeik]

you still need help?

the picture is that What u call A oil

 

[UWe9o12jkied91d]

Is that borosylicate?

 

[Sjeik]

No Its the finishing product, amfetamin free base, the picture What u see is after steam destillation we wash it with hot water. It Will seperate and Will be clear

 

[Sjeik]

Lol, u mean the seperation funnel. No i dont know What kind of material exactly, hard plastic if u ask me. They use it to make beer

 

[UWe9o12jkied91d]

Aha ok

 

[w2x3f5]

It doesn't look like oil or emulsion, it looks like you did something wrong

 

[Sjeik]

Jacked off And disposed in it

 

[Botsauto-Dutchland]

final liquid you mean bmk or a oil they both solve in dcm or there was water layer also ?

 

[Botsauto-Dutchland]

whats the final layer ph ? is it the ketone or A- oil when you have the a oil in dcm wash it with water and then separate. than add acid until low ph and amine goes into water after stirring. than you safe layer dcm. and basify the acid water with Naoh solution. you should see a top layer leave it for a day and separate.

 

[John Gotti]

Hi ive had bmk oils for long time now and there is a blocker in them they need to be activated or something. But is it easier to get the bmk powder 5449 and make the oil into A oils but how do u do that

 

[Sjeik]

If you convert it the right way, you Will receive a yellow/brownish coloured oil depending on wich reagent u use. We call that b oil. If you fail doing that it Will be a thick oil that Will turn milky afterwords. So its very important that you convert it the right way, or else your waisting your time and money

 

[w2x3f5]

There is free glycidate or sodium glycidate. The sodium salt is highly soluble in water and they use it for hydrolysis in hydrochloric acid, I have more doubts that all the sodium salt will react quickly with decarboxylation, it will quickly turn back into free glycidate. Free glycidate reacts perfectly in pure phosphoric acid, two important points in the reaction are to obtain a homogeneous mixture and the second nuance is the decarboxylation temperature.