Question 3cmc powder

ancelotti

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busy with the 3cmc syntheses I just took the oil with ph value 5.5 out of the freezer after 12 hours. but unfortunately there is no powder in it what could be the cause of this?
 
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ancelotti

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I did the acidify in acetone instead of water... What can i do to solve this ?
 

G.Patton

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How exactly did you do this? What is the reaction mixture volume and acetone you added?
 
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