Kannabidiolin (CBD) isomerisaatio psykoaktiivisiksi kannabinoideiksi

kitboy

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GqYXjsEBI7


Olin keittämässä CBD:tä ja lisäsin vahingossa NAoh:ta seokseen, luulen, että isomerisaatio pysähtyi. Muodostui 2 kerrosta, voiko joku kertoa minulle, mitä muodostui? Onko se hyvä tapa uuttaa THC-uutetta?

Käytän metanolia ja HCL:ää
 

G.Patton

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Hei, missä vaiheessa olet lisännyt NaOH:n?

Vastaus voidaan antaa HPLC-analyysin avulla.
 
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kitboy

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Kahden tunnin isomerisoinnin jälkeen muodostui öljyä, mutta siinä on epämiellyttävä haju, enkä tiedä, miten se puhdistetaan.
 

kitboy

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Kun Naohia lisättiin, kaksi faasia erosivat toisistaan ja reaktio taisi pysähtyä. Yritin pestä sitä monin tavoin, mutta en pääse eroon tuosta pahasta hajusta.
 

cvvvxa

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Uskon, että sen erottamiseen thc:stä voidaan käyttää erilaisia liuottimia, mutta en muista, mitä niistä. Missä kirjallisuudessa se on kuvattu, ja koska se on vihreä (oletan), myös jotkin kasvien epäpuhtaudet voivat hapettua.
 

kitboy

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Kumpi on parempi etikkahappo vai suolahappo? Minulla on öljy jäljellä inhottava haju, jonka teen puhdistaa sitä tai uuttaa puhdasta cbd loas metanolista
 

cvvvxa

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huoneenlämpötilassa olevaa tolueenia ja p-tolueenisulfonihappoa voidaan käyttää lähes puhtaaseen delta 9:ään, ja muut liuottimet, joissa on lämpöä, johtavat delta 8:aan.
 

cvvvxa

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tolueeni voi olla vaikea poistaa, mutta, 44h(48h johtaa hieman enemmän muuntaminen, mutta noin 10% delta8) sekoitetaan 10% ptsa ja tarpeeksi tolueenia liuottamiseksi, sitten workup
 

kitboy

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Kun lisäät NAOH:lla kyllästettyä vettä hapon vastapainoksi, en pysty poistamaan sitä kokonaan, ja jos lisään liikaa vettä, ylempi faasi muuttuu mustaksi. Miten voin tehdä uuton? Miten poistan hapon hajun? Yritin puhdistaa sitä tislatulla vedellä, mutta se ei toiminut.

Tarvitsen apua tässä asiassa

Minkä PH-arvon pitäisi jättää THC:lle? Voinko käyttää butaania tai tolueenia THC:n puhdistamiseen?
 

WillD

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Menetelmät, joissa käytetään katalyyttisiä määriä happoja, ovat vakiinnuttaneet asemansa paremmin kuin tässä aiheessa. Kun pTSA 10 % mol DCM:ssä (delta-8) tai HCl 0,05 % etanolissa (delta-9).
 

Dr. MMX

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voidaanko käyttää eri alkoholia kuin etyylialkoholia? ehkä ipa sen sijaan?
voidaanko käyttää hcl:ää?
 
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Irving Langmuir

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Luulen niin, kunhan reagenssit ovat liukoisia. HCl:ää voidaan käyttää happokatalysaattorina.
 

WillD

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Liuottimen ja hapon määrän muuttaminen muuttaa suuresti tuloksen koostumusta
 

kitboy

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Mielestäni on parempi käyttää metanolia
 

Kvadprime

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I love vape with TGK ... I think I can do:

1. We carry out isomerization in ethanol with acetic acid for 12-24h.
2. After - we evolve all ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?
 

Kvadprime

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I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?
 

WillD

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You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.
 
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Kvadprime

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Hmmm... Of course!
And question

If I use AcOH in concentration about of 70-80%, It get to start isomerisation?

Now.... I can't get or make 100% acetic acid((
 

WillD

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Then you need 7.5 (70%) - 6.5 (80%) mL of acetic acid soln. per ~100mL of ethanol (approximately).
Excess ethanol is necessary for the reaction to go well.
The resulting solution will take 5-10 g of cbd powder, nothing more.
Heat up to 70*C and boil at least 2 hours.
Dilute with water and collect the resulting oil.
You can write us about your results after.
 

Kvadprime

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Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!
 

WillD

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The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.
 

Rabidreject

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I have wanted to do this for ages but have been holding off as I don’t have p-tsa, however, if d9 is generally done with a catalytic amount of HCl, that would be MUCH easier.
Is it literally a case of chucking it all in, letting it react for ages at RT (12-24h I think I heard), quenching, extracting?

Seeing as THC is by far the drug I use the most, it would make sense for edibles or whatever. Doubt I would want to vape it though. Never was a huge fan of vaping distillate as it just screws my tolerance.

It looks pretty easy though
 

Kvadprime

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Yes, it looks simple. That's why I want to try it!.. I'll write when I do it, there will be another report
 

WillD

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If you use HCl for conversion, then heating is required.
 
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