Kanabidiola (CBD) izomerizācija līdz psihoaktīvajiem kanabinoīdiem

[MuricanSpirit]

Tāpēc tagad sajaucu 20 g pārtikas sodas (pirms tam es tik un tā sačakarēju, tad kāpēc gan ne turpināt). Maisīju ar maisīšanas stieni apmēram 1h. Nebija pietiekami daudz etanola, lai atdalītu, tāpēc es pievienoju (pirms maisīšanas) 40 ml etanola.

Ar šļirci atdalīju virsējo slāni - smieklīgi, ka tas bija 50ml, tāpēc apmēram 13ml joprojām ir iesprūduši sodā - un iemetu to katliņā (zemākais karstuma punkts 56°).

Drīzumā šo sūdu izsmēķēšu. Joprojām smaržo, bet daudz labāk nekā iepriekš.

 

[mycelium]

Just so you know, after the reaction, it is distilled again or maybe twice, in order to clean it up and remove reaction byproducts

 

[WillD]

Parasti tīrs CBD pulveris pakļaujas izomerizācijai, es nezinu, cik tīrs process notiek ar eļļu

 

[mycelium]

I think anyone who is making it for sales should use isolate, and DISTILL END PRODUCT AT LEAST ONE TIME

 

[PossumKid]

Vai jūs varat viņiem pajautāt, kāda tīrības pakāpe tā ir?
Parasti, ja tas ir izolāts, tam vajadzētu būt labam, bet tas, ka tur ir rakstīts arī "plaša spektra", mani nedaudz mulsina.

 

[mycelium]

Broad spectrum means all cannabinoids, not isolated like CBD isolate

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rafa]

what substitutes can i use for Et2O?

 

[WillD]

We need more details to a specific task.

 

[Rabidreject]

Yeah, I’m probably going to end up just running it a few diff ways, I said HCl purely because I have some lol
I saw someone synthesise some p-tsa the other day and it was far less violent than I’d expected so I’ll probably whip some of that up and also give the citric acid method a go also.

 

[Rabidreject]

In terms of vacuum distilling out the product for purification, I assume I’ll be able to vacuum distil to separate the d9 and d8 right? If I use a collumn?

 

[mycelium]

@Rabidreject No sir, they come out at same temp.
It's damn near impossible, even with chromatography and lots of solvent, and this is from the professionals over at future