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Synthese van 4'-methylpropiofenon uit tolueen door Friedel-Crafts reactie (schaal 1kg+)

NovicechemistEU

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Tomorrow I'm starting the big day synthesis with a small batch.
I wanted to start with a small batch for my first try.
1.08 mol 100 Gr 95.2 mL propionyl chloride
1.12 mol 150 Gr: AlCl₃
2.81 mol 300 ml 261 Gr Toluene
I can use 50 ml more toluene. 350 ml
Toluene of 99.5% purity was dried and then distilled under vacuum. We follow the advice of the masters :)
 
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Smokesalot99

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Can you replace propionyl chloride with propionic anhydride for reaction?
 

The-Hive

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try it and let us no do it on a small scale then compare it to using propionyl chloride
 
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