4MMC/MEC large crystals

Sergey Kush

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4-MMC in dry methanol. T 15-20C, 1 week
 

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Only water is no posible with only water get like this crystal
 

Sergey Kush

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IPA for crystallization 4-mmc is bad. Methanol is the best
 

Sergey Kush

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It is possible. 1g of 4mmc to 0.7ml of water at boiling. Then just leave in cold place for 10-12 hours
 

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Im made with ipa and made like you see you made 3 week because you use to much water simple
 

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In acetone you can do ipa pure wodka from shop is much ways
 

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How much methanol You give for 1 g powder.
 

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This crystals are soft or hard?
 

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How you guys clean the freebase? Only water or NaOH also or Sodium Bisulfite solution?
How long you cook the DCM with 2b4m and at what temperature?
 

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This crystals are very hard. you must use a thick knife or screwdriver to pry these crystals away from the glass container
 

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after the reaction of 2b4m with methylamine in DCM, the free base of mephedrone is washed 2-3 times with an equal volume of water. the reaction with methylamine lasts 4 hours at a temperature of 32-36C. do not bring DXM to a boil (38C), as DHM hydrolyzes when boiling, the free base will be heavily contaminated. if the temperature/time is observed, the free base will be very clean.
 

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7-8 ml for 1 g powder and You let this to evaporate all methanol?
 
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