Methamphetamine Synthesis From P2P Via Al/Hg

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Hello can i use an aluminium foil of 12um ? And also can the methoxy phenyl acetone work well
 

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Yes on the 12um aluminum foil, You can use aluminum pellets to make the al/mg doesn't have to be foil. need to elaborate more on the Methoxy phenyl acetone?
 

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When filtering how dense filter should i use?
 

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Just use a Buchner funnel, filtration paper and a vacuum pump.. You can't make quality without the proper equipment.
 

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Ive been using 52 micron coffee filter, but its kind of slow and can place ~100g per filter
 

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Please, friends and teachers, Ican I wash the evaporated crystalized reaction mixture with ethyl acetate, please I need expert advice and what is best temperature for evaporation of the oil reaction mixture
 

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I really need your assistance, in my second attempt to produce meth using P2P, am at final stage of evaporation to crystalization and this is evaporated crystals picture, Please can I wash with ethyl acetate or diethyl acetate,, and please how do I convert it to big rocky crystals, I really need help friends in the group,
 

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G.Patton

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Hello, you can wash it with acetone. Then, you can just recrystallize it or separate isomers in order to make big crystalls of d-meth. Tutorials are posted on the Forum. (with video)
 

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Basify, extract preferably with hexane and wash with brine, then let stand salt out.
 

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one question, after some tests with small scale it looks like it will work fine.
but i will do a bigger batch next time and now i am a little bit confused after reading infos on different places.
The reductive alkylation with Al/Hg and P2NP to Amphetamin this way i know for many years, from this point i cant understand this :
from oncle fester.

onlcel fester says:

for ME i cant belive that he do this in a 3l flask. In a 3l flask i can maybe do 30g P2NP batch in colder days. But he says something from about 340ml P2P.
is this possible ? Is the reaction so much gentler then with P2NP ?
 

G.Patton

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Hello, yes, it is less exothermic than P2NP reduction. But I also don't recommend to make 340 ml P2P reduction in 3L flask. In my opinion, it's too much.
 

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The big difference between the reactions of reductive amination and the reactions of the reduction of nitro with a double bond.
 

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Will methamphetamine be obtained without evaporation by producing HCl gas through sodium chloride?
 

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I tried to make small amount of methamphetamine by mixing P2P, methylamine HCL free base, sodium chloride and ethanol in aluminum mixture, then filtered after 3 hours, got methamphetamine free base, I made HCL gas by mixing NaCl and H2SO4. Added to the methamphetamine free base, there was no reaction with any of the substances in the methamphetamine free base.
 

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I have mercury nitrate monohydrate, can I use it in this? Or buy another mercury 2 chloride ?
 

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Yes, Mercury II Nitrate monohydrate works but adjust ratio.
 

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can i replace diethyl ether in this method??
 

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Hello, at present, methylamine (74-89-5) in my area is tube. Can I use methylamine hydrochloride (593-51-1) instead of methylamine?
 

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Hello, can I use 1000 purpose aluminum powder instead of aluminum foil?
And can ether be replaced with petroleum ether?
 

wael gph

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The powder is not good and does not make amalgam as it generates hydrogen at a high speed
Aluminum foil is effective as it helps in transferring electrons as well
 
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