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The leuckart is so simple, but the yields are absolutely garbage.
If people could figure out how to increase yields, this would help the clandestine chemistry community so much.
Apparently magnesium chloride can be used as a catalyst, from what I've gathered online, maybe that will help yields a few percent points.
If people could figure out how to increase yields, this would help the clandestine chemistry community so much.
Apparently magnesium chloride can be used as a catalyst, from what I've gathered online, maybe that will help yields a few percent points.
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I don't have the link on hand, but I have read amongst the Rhodium archives that the use of a Dean Stark trap filled with water increased yeild. By removing water as it was generated but keeping the trap full gave a bette result.
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A Brief Review: Advancement in the Synthesis of Amine through the Leuckart Reactionby Qasim Umar and Mei Luo
There you go, massive increases in yield and also speed.
A Brief Review: Advancement in the Synthesis of Amine through the Leuckart Reaction
This review presents a summary of reactions that take place during the “Leuckart-type reaction”. The significance of, as well as recent advancements in, the synthesis of amines through simple and inexpensive methods using readily available raw materials is discussed. This review includes all...
www.mdpi.com
There you go, massive increases in yield and also speed.
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I don't understand any of the shit in that paper, please break it down. Also how high is the yield with this, what chemicals need to be used and how fast does this speed shit up? If possible just make a diagram plz.
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Ok how much yeild increase is it and is there any synthesis of this done with ratios of Chems