VAPE LIQUID THC

[Curiousonion]

Ok, will do it tomorrow.
It's a very simple reaction and all the chemicals are easy to obtain. Gives a 86% d8. Yield is close to 100%

 

[Curiousonion]

To a 5liter 2 neck flask add

1:1 ratio of cbd isolate /methanol (1 liter methanol 1 kilo cbd)
Bring to 63c
Add 1% p-acid
Reflux for 60 minutes (gentle)

Let cool down.
Add 2 liters dcm

Do water wash
Bicarb wash
Another water wash
Separate water from dcm

Distill dcm
Short path distillation to get clean product

 

[GOUPIL]

thank you so much for your help!

i don't understand well theses parts :
Bring to 63c
Add 1% p-acid

Can you give me your mail in case of the forum is down or crash?

 

[Curiousonion]

You mix the cbd with the methanol and you raise the temp to 63c. Once it reaches that you add 1% p acid by volume to the cbd then you reflux it for an hour

 

[GOUPIL]

thank you for all your post! i am trying something and i will keep you in touch !

 

[Curiousonion]

Welcome

 

[CristalKing]

What is p-acid ? ( phosphoric acid ??) and how many delta 9 and delta 8 is after this reaction ?

 

[Curiousonion]

It's p-Toluenesulfonic acid. 86% delta 8. No delta 9.
To get d9 you need to use a different method.

 

[Pan Cyga]

You can find the same set on alibaba.com probably for a few hundreds dollars or something.

 

[Curiousonion]

What set?

 

[Pan Cyga]

distillation kit

 

[Curiousonion]

All equipment should be bought from china. Saves you a ton of money

 

[GOUPIL]

how much is the good price for a distillation kit?