4MMC/MEC veliki kristali

Sergey Kush

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4-mmc v vodi.
 

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infochem

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Pozdravljeni, samo voda? Prosim, povejte mi delež ,temperaturo in čas.
 

Heineken

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Moj novi način, ki je kristal zdaj so jebeno trdi in je zelo težko trk s kreditno kartico in so resnično veliki :)✓ ✓
Zdaj so rastejo je 1 dan
 

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Heineken

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Za današnji dan lepo ledeno čisti kristal.
potrebujem suho 1h in to je vse pripravljeno za uporabo:)
 

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antrax

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what´s the point of crystals and not leave it in the hydrochloride form? Mislim, da kristala ni mogoče posrkati.
Ali mi lahko to razložite, hvala!!
 
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xile

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Ste na pravi spletni strani? Of cours the crystals where grindet and snored or crystals where eaten.
 

Goku

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na prvič izdelano ni tako slabo :)
 

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Goku

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Da bi dokazali, da je mogoče narediti čudež.($)
 

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Gordon Ramsay

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Zdi se, da je to postala nit za objavljanje slik lepih kristalov 4MMC :)

VuCILaxYEn
VlKJITtup4
 

Albert A

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Dragi prijatelji, ali kdo ve, kako iz 4-mmc izdelati tako lep kristal (kamen) ?
 

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Gordon Ramsay

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Zdi se mi, da gre za kokain :D
 

Albert A

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4mmc je bil izdelan v obliki, ki je zelo podobna kokainu.
To je bistvo.
 

Gordon Ramsay

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Zelo zanimivo :) No, rekel bi, da je to popolnoma prečiščen stisnjen prah, kot to počnejo s kokainom, mislim, da
 

Eureka

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Tukaj je fotografija 4MMC v vodi, segreti do nasičenosti pri 95 stopinjah v loncu, nato pa postavljeni v izoliran hladilnik z dodano vrelo vodo kot kopeljo.

Hladilnik je zaprt in pokrit s spalno vrečo. Odprt po 24 urah.

Če je raztopina čista, so kristali široki od 0,8 do 1,2 cm.
W01M64hd35
 
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Metoda postopnega ohlajanja deluje na enak način kot vse druge. Topnost 4mmc pri nižji temperaturi pade in kristal začne rasti. Čim počasneje se temperatura spreminja, tem večji je kristal.
Pomanjkljivost je, da tudi po končani kristalizaciji nekaj 4mmc ostane v vodi. Zato je bolje uporabiti dve topili.
 

Acidosis

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Velik odstotek vode in manjši odstotek topila bosta ustvarila popolne kristale, topilo pa bo zadržalo in shranilo preostanek izdelka za poznejšo ekstrakcijo.
RugKdlCsiI
 

HerrHaber

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Rentgenski difrakcijski vzorec bi bil bolj prepričljiv (takih 4MMC nisem videl od leta 2010, zato vem, da so lahko takšni, vendar jih osebno nikoli nisem pridobil). P.S. Nimam nobene dejanske usposobljenosti za interpretacijo podatkov XRD...
 

Gordon Ramsay

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Zakisano v aeq. plast, očiščeno v aeq. plasti z DCM in kristalizirano z raztopino 2:1 voda:aceton 🐱 💎

OxBLdSpQ40
 
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