Metoda stresanja in pečenja za 4mmc

kinshasa99

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Ali je kdo preizkusil metodo stresanja in pečenja za proizvodnjo 4mmc z DCM?
Katera so s tem povezana tveganja?
 

Netflix

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Da, lahko uporabite dcm toulen ali benzen
Morate izdelati
~2xJar
~1xTape
~2xPlastična vrečka
~1xtočka
~2x brizga 100ml \ 50ml
~Stara majica

Whis je tisto, kar potrebujete za opremo:)
 

Netflix

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Da, lahko uporabite dcm toulen ali benzen
Morate izdelati
~2xJar
~1xTape
~2xPlastična vrečka
~1xtočka
~2x brizga 100ml \ 50ml
~Stara majica

Whis je tisto, kar potrebujete, obrazec
 

Netflix

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Kemikalije
{100g}
2-bromo-4metilopropiofenon
{500ml} dcm toulen ali benzen
{200ml} metilojamin 40% v vodi
{3x300ml} poceni voda iz trgovine brez plina!!!
{500ml} tehnični aceton iz trgovine za gradbeništvo
{55ml} kislina hcl 35%-38% če imate 31% kisline, potem potrebujemo več za uporabo
To je vse, kar potrebujemo, da naredimo na ta način:)
 

ymaaah

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če želim izdelati večjo količino, na primer 1 kg, moram reagente pomnožiti z 10 ect...?
 

ymaaah

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Rekli ste "poceni voda iz trgovine", vendar vam ni treba uporabljati destilacijske vode? Demineralizirana voda je lahko dobra?
 

41Dxflatline

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Pitna voda je običajno obdelana z reverzno osmozo in dekontaminirana z UV-žarki.
 

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2-bromo-4-metilpropiofenon v
DCM
Korak 1
 

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Benz88

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Zakaj vreča? Ali lahko pojasnite več, prosim :)
 

Netflix

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za popolno zaprtje kozarca. Ko nalijem metilamin, plin ne more uhajati, nato pa poleg tega kozarec zatesnim s trakom.
 

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antrax

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Ali je bolj učinkovito zapreti posodo, da plini iz vodne raztopine metilamin 40% ne uhajajo, ali pustiti posodo odprto, da plini prosto uhajajo?
Hvala!!
 

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Naslednji korak
Prevzemite
2-bromo-4metilopropiofenon 100g\50ml v dcm 500ml= 550ml
In monometilojamin 40 v vodi 200ml
In vzemite večji kozarec 750ml
2b4m v dcm nakapljajte v večji kozarec
in kasneje monometilojamin
uporabite vrečko in tabe ter stresajte 30 minut
 

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V dcm dobite 4mmc proste baze, na vrhu pa imate monometiloamin
Vzamete monometilojamin in spustite vodo ter kasneje sperete, imamo
olje 4mmc freebase
 

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Dexterror

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Imam vprašanje, zakaj vzamete zgornji del raztopine, da jo segrejete, spodnji del pa je 4mmc freebase? Zakaj potem vzamete zgornji del?
 

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Prosta baza in voda na vrhu
 

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Netflix

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Kasneje uporabimo kislino hcl 35%-38% 55ml in 500ml acetona
250ml acetona kanemo v olje in zmešamo kislino z acetonom in vse kapnemo v prosto bazo z acetonom in hitro zmešamo les in počakamo 30min in dobimo ....4mmc hcl :) Ph 6\5,5
 

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Veliko ljudi me sprašuje, kako im dobim takšno barvo olja preprosta, če je čista 2b4m dobiš takšno barvo olja
Naslednji test :)
 

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Ko padeš na hitro kislino, se ti rodi mef in je kot to olje, vendar
Tokrat dobimo lepo belo mleko
 

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ymaaah

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Pozdravljeni, Netflix :)

ali imate na voljo sintezo v pdf formatu? :)
 

Methylamine

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Pozdravljeni, ali je kdo preizkusil ta recept za metodo stresanja in pečenja?
 

StarWars

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Videoposnetek stresanja in pečenja

 
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HerrHaber

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Kratek prevod dogajanja v videoposnetku je lahko v pomoč ... gre le za radovednost
 

ymaaah

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kakšen je donos? Predvidevam, da ne veliko...?
 
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