Sinteza amfetamina iz P2NP prek SnCl2 in Zn

Bigballen

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Koliko želene kisline je treba dodati na koncu?
 

blacky2340

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Na 1 ml koncentrirane žveplove kisline v razmerju 10:1 nalijte 10 ml acetona. S pipeto ali brizgalko počasi kapljajte raztopino, dokler ne dosežete pH 5,5. Če je prekislinjena, dodajte več proste baze, če je močno prekislinjena in se spremeni v tekočino, potem v a/b in ponovno kristalizirajte.
 
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ActionAyi

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Razmišljal sem tudi o toulenu, vendar mislim, da je razlika v gostoti premajhna, mar ne ?
 

sandman

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Mislim, da to ne deluje. Upam, da deluje, in bom moral poskusiti.
 

TucoSalamanca.

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Upam, da ti bo uspelo, kolega, meni ni.
 
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mithyl2

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metodo z borohidridom sem uporabil že večkrat in brez uspeha. najbližje sem bil, ko sem naredil približno 0,2-odstotni izkoristek amfetamina. vendar je bil pravi. zelo potrebujem, da to deluje, in to me popolnoma spravlja ob pamet. sporočite nam, kako gre dcm.
 

TucoSalamanca.

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Pisal bom, prijatelj, ne zamudite svojih molitev, da bo ta sinteza lahko uresničena, hvala. ❤️
 

TucoSalamanca.

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Danes nisem mogel sintetizirati, to bom storil jutri in o tem poročal.
 

ActionAyi

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Ali obstaja kakšen drug način za pridobivanje izvlečka kot DCM ?
Morda n-heksan?
 

August

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Pozdravljeni prijatelji, ali pri tej reakciji ne nastane samo feniletilamin (PEA) ali sem samo neumen (velika možnost)
 

Amin. M

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Pozdravljen, moj prijatelj
prebral sem vaš komentar in užival v njem
Kako ste dobili čisti amfetamin (v drugem koraku)?
Prosim, svetujte, katera metoda pridobivanja amfetamina je boljša in ima na koncu večji odstotek čistosti
In da je surovine nabavil prek trgovine
(nimam profesionalnega laboratorija)
 
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