Isomerisering av cannabidiol (CBD) till psykoaktiva cannabinoider

[MuricanSpirit]

Så jag blandade nu 20 g livsmedelssoda (jag klantade mig ändå tidigare så varför inte fortsätta). Blandade det med en omrörningsstång i cirka 1 timme. Det fanns inte tillräckligt med etanol för att separera så jag tillsatte (före omrörning) 40 ml etanol.

Tog bort det översta lagret med en spruta - roligt, det blev 50 ml så ca 13 ml sitter fortfarande fast i läsken - och slängde det i en kokkärl (lägsta värmepunkt 56°).

Kommer att röka den skiten snart nog. Det luktar fortfarande men men mucher bättre än tidigare.

 

[mycelium]

Just so you know, after the reaction, it is distilled again or maybe twice, in order to clean it up and remove reaction byproducts

 

[WillD]

Vanligtvis lämpar sig rent CBD-pulver för isomerisering, jag vet inte hur ren processen går med olja

 

[mycelium]

I think anyone who is making it for sales should use isolate, and DISTILL END PRODUCT AT LEAST ONE TIME

 

[PossumKid]

Kan du fråga dem vilken renhetsgrad det är?
Om det är ett isolat brukar det vara okej, men det faktum att det också står "bredspektrum" gör mig lite förvirrad.

 

[mycelium]

Broad spectrum means all cannabinoids, not isolated like CBD isolate

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rafa]

what substitutes can i use for Et2O?

 

[WillD]

We need more details to a specific task.

 

[Rabidreject]

Yeah, I’m probably going to end up just running it a few diff ways, I said HCl purely because I have some lol
I saw someone synthesise some p-tsa the other day and it was far less violent than I’d expected so I’ll probably whip some of that up and also give the citric acid method a go also.

 

[Rabidreject]

In terms of vacuum distilling out the product for purification, I assume I’ll be able to vacuum distil to separate the d9 and d8 right? If I use a collumn?

 

[mycelium]

@Rabidreject No sir, they come out at same temp.
It's damn near impossible, even with chromatography and lots of solvent, and this is from the professionals over at future