mdp2p

Hello ,how is everyone, I want to know if here are some mdp2p vendors

What would be the best and preferably simple solution for purifying MDP2P? If my PMK oil is currently brown/dark yellow, would that cause problems in subsequent reactions, or would the impurities just remain in the final product?

let me preface this by saying yes, i know @WillD made a lovely thread, but these links go "further back" and start the process earlier. his synth starts with MDP2P which is in the second to last/last links on this list. i just wanted to put that out there so this doesn't get considered redundant...

Previously, NaBH4 was used for production, but to expand production, I want to change the method to H2/PtO. Does anyone know that the metal can be replaced by Pd? Does anyone provide teaching services to help me build a 1-ton production line? The amount can be discussed in detail.

After nabh4 addition is complete and mixed for a few hours after can you let the mix sit for a few hours and the freebase oil layer will rise to the top and can be seperated? this eliminates the need for dcm or toluene extraction but does effect yield.

Is there anyone that is speaclised in synthesis using fried-crafts adylation ? I would like to send them a theoretical synthesis but don’t want to post it if it’s not correct .

I have been out of the game for years.. i ran a operation for a while that i did 250g batches using Al/Hg method. I have made mdp2p all the way from shaving sass root bark until i discovered PMK glycidate. BIG game changer lol. Anyways ive found myseld getting back into the action again and have...

and with 1 liter of PMK, how much MDMA can be obtained? Thank you, all!! :)

An OTC MDMA synthesis route. Even though many routes exist for the synthesis of MDMA but in some routes the precursors are not easily obtainable (like safrole,palladium catalysts,etc), in some routes scalability is an issue (like if you start from vanillin/eugenol as a precursor scalability...

I see most buy pmk ethyl glycidate (28578-16-7) and then convert it to PMK (4676-39-5) but I see that converting from one substance to another is complex, and I was curious if anyone has been able to successfully and without being scammed, buy the PMK directly, without the need to buy an...

I would like to know how to convert from PMK ethyl glycidate to MDP2P, thanks everyone!

in the synthesis of piperonal and nitroethane, Could I replace it with nitromethane?

Hello guys I have a question: There was a video of a complete synthesis of MDP2P in the category video. But now it is gone! Does anyone know the reason why and where I can find or download it from? Thank you very much for any kind of help.

This is so frustrating. I’ve followed processes to the T and first i yielded a resist clear oil, this second time distilling under vac not exceeding 106c I yielded a totally clear liquid which smells like solvents. idk anymore. Here’s some pics of after adding the pmk oil to 300 ml of naOH...

Hi, This is my first big project in organic chemistry. So your help is welcome. My theory is isolate a piperine from black pepper and convert to a piperic acid. And reaction with potassium permanganate cause a oxidative cleavage and makes piperonal and piperonylic acid (Is possible this acid...

Introduction The following method shows that the NaBH4 reduction actually is superior to all other common routes used in clandestine chemistry and this method allows to scale MDMA synthesis unlike aluminum amalgam reduction. The method is quite simple, it doesn't take expensive equipment...

Hello, I've recently come across a local connection who's able to provide me with [~92%] PMK oil. I've been reading various PMK -> MDMA synth guides on here and other forums, however I'm finding myself asking more questions than the guides are answering. Somebody recommended I try Bright...

Introduction These precursors, are controlled or regulated substances in many jurisdictions. The use of uncontrolled precursors therefore offers clandestine laboratory operators a strategy to reduce the risk associated with detection. Catechol (1) is a common chemical reagent that is synthesized...

Reaction scheme: Reagents: Methylamine 40% aq (cas 74-89-5) 2 ml; Ethanol (EtOH) 5 ml; 3,4-Methylenedioxyphenylpropan-2-one (MDP2P; PMK; cas 4676-39-5) 2 ml; Adams' catalyst (PtO2; cas 1314-15-4) 0.05 g; Distilled water 165 ml; Hydrochloric acid (36% aq HCl); Dichloromethane 450 ml; Dodium...

Reaction scheme: Equipment and glassware: 100 ml round bottom flask; Retort stand and clamp for securing apparatus (optional); Reflux condenser; Heating plate; Funnel; Syringe or Pasteur pipette; pH indicator papers; Beakers (250 mL x2, 100 mL x4); Vacuum source; Laboratory scale (0.01-100 g...