ASheSChem's Amphetamine Trials and Experiments

BongMan

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it is L or D... or mixture ...?
 

yin-yang

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You could try distilling out A-oil, that should get rid of impurities
 

ASheSChem

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this is not bad for the amphet?
 

ACAB

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The sulfate salt is stable, what should happen? I also like to use a heat lamp, which also produces approx. 60 °C.
 

ASheSChem

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ideally i need to do an acid base extraction for purifying

okok; it is often advised to keep/store it at room temperature or in a cool place; I was afraid of heat sources :p
 

ACAB

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Yes that is also true, but you are not supposed to store it at 60°C for weeks, but dry it for one hour. Is also just a suggestion how it goes faster, under vacuum drying is also good and fast.
BTW if you dry the sulfate with a lamp you can see the impurities, they become slightly yellow reddish, but no idea why, you can just see it, clean sulfate is pure white.
 

ASheSChem

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i found this... you think is ok ?
RWqiFpVAKM
 

Mclssmxxl

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i found this... you think is ok ?
That’s the stuff, yeah.Very good solvent.
 

ASheSChem

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Great! is it really certain?
I was sure to buy it for nothing ;)

anyone else who confirms? :)
 

ACAB

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There are many mixtures of petroleum ether, lighter fluid Benzinum medicinale, Ligroin, White spirit, Naphtha or special gasoline. It is important that the boiling point is between 40 and 60°C, this should be known. A separation is also possible with the others, but an evaporation is difficult. It is best to ask the dealer for a safety data sheet (he must have it) or check in advance on the website, in the data sheet is the boiling point in any case.
 

ASheSChem

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i don't find the boiling point...
for you i can't use it ?
 

ACAB

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As it looks yes. I think you bought petroleum for lamps like ----> wiki1 , but you need petroleum ether like ---->wiki2 with a boiling point of 40-60°C.
 

ASheSChem

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ACAB

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It is not so bad, look, a nice petroleum lamp in the evenig when sun is sinking is also a nice experience :D
 

ASheSChem

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Otherwise, today I was able to see that a 4/5 day nitrate mercury liquid kept in the fridge in an amber vial works very well;)

also, I made aluminum balls a little bigger than the first time, and I washed with 3x500ml H20 to remove the nitrates.
like that the thermal reaction was much less violent than the first time when I added the P2NP
 

ASheSChem

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the result of today was filtered (max i can, need to sleep :p); and i put the cream in my incubator
but this time... he doesn't smell speed !, only isopropanol actually not dry^^

soo the speed odor come from when we don't wash nitrate? ... it's scary when you think it's the classic smell of "street speed"

8DmuBISGH7
 

Mystery_chemistry

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I have the same problem . after adding acid in IPA, squeezing it through the material and putting it into the freezer, the product did not want to dry ... it looked more as if it was sweating ... And to a large extent this sulphate escaped somewhere, leaving a small yield, slightly smelling of alcohol. I will add that I did not have time to do everything myself and I had to buy freebase amphetamine oil. overall it looked very good. transparent with a delicate fragrance known to amphetamines. I obtained the pH of 5 after adding 250 ml of sulfuric acid solution in the ratio 1: 4. 180ml: 720ml. I also added 1/2 volume IPA to the oil ... does anyone have any idea why the yields were so small?
0XRyLBk7hM
 

Mystery_chemistry

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BWDxMVhRv3

the product was wet all the time I added fillers and it made popcorn ...
 

MadHatter

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You can't expect the product to dry in the freezer. heat it under a lamp to evaporate solvents. I can also assure you the sulphate didn't escape, the solvents escape. If you didn't dry the amphetamine sulphate enough, it's dirty. Then you added fillers to trap the impurities in there and make your product even dirtier. Also, it's very difficult to annswer anything about your yield if you don't tell us what your yield was ...
 
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