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Dear Mr.
Use L tartaric acid to separate the free base according to your method.
I got a chewing gum-like substance while stirring, and once I stopped stirring everything turned into a very hard white solid. A whole piece.
Is this correct?
Use L tartaric acid to separate the free base according to your method.
I got a chewing gum-like substance while stirring, and once I stopped stirring everything turned into a very hard white solid. A whole piece.
Is this correct?
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Yes
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- By btcboss2022
It won't turn liquid the liquid is mixed with the hard solid you must crush it to vacuum filtration and get the liquid.
About freebase yield from p2p is ok if not steam distilled p2p used.
About freebase yield from p2p is ok if not steam distilled p2p used.
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Dear Mr.
I used L tartaric acid to separate the free base. Vacuum gives liquid. Alkaline PH-13. Free base is obtained.
Stir the free base. Join HCI. PH value -2. I wanted to adjust the pH to -3. But the pH suddenly dropped. I'm careful to add very little HCI. The pH value has always been around 7 in the beginning. Then suddenly it drops to -2.
Heat to 130°. Pour into a container with 10 volumes of chilled isopropyl alcohol. A lot of powder immediately appeared in the container. Shouldn't we get crystals?
What did I do wrong?
Sir, please help me.
I used L tartaric acid to separate the free base. Vacuum gives liquid. Alkaline PH-13. Free base is obtained.
Stir the free base. Join HCI. PH value -2. I wanted to adjust the pH to -3. But the pH suddenly dropped. I'm careful to add very little HCI. The pH value has always been around 7 in the beginning. Then suddenly it drops to -2.
Heat to 130°. Pour into a container with 10 volumes of chilled isopropyl alcohol. A lot of powder immediately appeared in the container. Shouldn't we get crystals?
What did I do wrong?
Sir, please help me.