Fenethylline (Captagon) synthesis

MadHatter

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Thank you for an excellent write-up as usual!
But I can't really see the point of the drug itself? Why ingest a prodrug that gives you a minor amount of speed and a pretty useless asthma medication? Theophylline has no psychostimulating effects I'm aware of, and I know the medicaton quite well.
 
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41Dxflatline

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You'll never been a middle eastern warlord with that attitude
 

Mo0odi

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Mo0odi

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Captagon has a very large effect and strength, like methamphetamine. It increases strength, alertness and euphoria. It is the ideal substance for warriors in the Middle East.
 

Mo0odi

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It does not cause harm to the body like methamphetamine

Unfortunately, there is not much information about its synthesis
 

cyb3r0

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And the other point here, do you leave it here at a certain temperature?
 

G.Patton

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1,2-dichloroethane boiling point (~83 deg C), read topic about Reflux please
 

cyb3r0

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Does water or alcohol need to be placed here for the reaction to take place for four hours, or does it react without that and does it need a condenser?
 

G.Patton

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You don't need to add anything else. Yes, you have to use reflex condenser.
 

cyb3r0

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Thank you so much
 

cyb3r0

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In the oil bath, what type of oil is used, and what is the required temperature?
 

G.Patton

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Mineral oil for oil bath
 

cyb3r0

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My question here is, are the ratios correct here, the kilogram and the milligram for both substances? Thank you
 

G.Patton

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These are grams, I fixed it. Also, you could calculate it by moles.
 

Mo0odi

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Hello
I want to know more
What is meant here by derivative (3)
 

G.Patton

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Can you match the number (3) with the number (3) on the reaction scheme?
 

Mo0odi

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Hello
I want your help
How do I make this solution, what is the percentage of acid in the alcohol, and what type of alcohol is used here?
 

G.Patton

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About what are you talking about? EtOH.
 

Mo0odi

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I mean, how can I make this solution, what is the method☝️
 

G.Patton

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Sorry, I don't understand your request. Reformulate it clearly please.
 

Mo0odi

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I mean in [method 1-2] there is a hydrochloric acid (hcl) alcohol solution.

My question here is how can I make this solution
 

41Dxflatline

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You literally just mix them together. I will simplify it for you, if you want a 4% solution get 100ml of your alchol and add 3.6ml of alcohol to it. assume 1% of concentration is 0.9 in 100ml and you will have no trouble.
 

Mo0odi

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Thank you
 
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