Methamphetamine Synthesis From P2P Via Al/Hg

[Jordan Belfort]

Why no-where bubbeling occurs in hexane? And washing with hot water with NaCl and baking soda take alot of impurities.

Nevertheless if you use methanol instead of IPA you can do a direct extraction from the reaction mixture after adding lye with hexane.

 

[Jordan Belfort]

Also if you use nitromethane instead of methylamine you don't need to do coolin, plus you can distill and reuse your methylamine source. Less waste and less coste

 

[Jordan Belfort]

I am now checking if it's truly dextro when I make crystal from it. Once crystal is made I might put here. I must also mention I don't have the correct ratios yet I need to do more reactions

 

[Jordan Belfort]

after vacuum destillation i must also do liquid liquid extraction with acid base if you want to put dry hcl gas in it else you must put freezer. i found out harsh way.

 

[wael gano]

This picture indicates the reaction of nitromethane reduction with hydrochloric acid and tin metal
To produce methylamine gas

 

[Jordan Belfort]

Actually it's with magnesium shavings and some complex to make super grignard

 

[Jordan Belfort]

you worked with nitromethane before ? I have problems isolating the product that I will probably acified it in the future with citric acid and then vacuum distill all of, and from there one add lye to basify it again and the further vacuum distill the base (and water then ofcourse) and then extract distiliate with hexane and bubble dry HCL gas through it.

Or just freeze it and recrystallize it with IPA.

 

[minnimus]

Can you please explain how to use nitromethane instead of methlamin
In this reaction?

Is it possible do
Use RC fuel meaning 10% nitromethane 90%methonol and mix it with the rest of the recipe?

 

[BlueDex]

Try using non-toxic Aluminum Galinstan amalgam.

 

[neoking8]

thank you for the advice. Can anyone confirm if it's good to replace Al/Hg?

 

[Jordan Belfort]

With ultrasound you can activate Al foil, I added also gallium chloride when making but reaction didn't proceed I think as it should but once you add lye you get instant vulcano reaction (enjoy the high)

 

[BlueDex]

Ultrasound only works for grignard reactions to activate magnesium. Don't add sodium hydroxide! If gallium chloride doesn't activate the aluminum foil, try Galinstan (Gallium Indium Tin alloy). You heat up Aluminum foil pieces and Galinstan in a crucible and have a 90%-95% Aluminum and 5%-10% Galinstan. You dissolve P2P (Phenyl-2-Propanone) and ethylamine in ethanol and hydrogen oxide (distilled water, H2O) and add Aluminum Galinstan (Al/GaInSn) and then heat it for a few hours to get Ethylamphetamine. Using methylamine will make methamphetamine. Using Ammonia will make amphetamine, though in lower yield. Devil Springs and Everclear have high ethanol content. The Galinstan is recoverable and reusable.

 

[BlueDex]

You don't add sodium hydroxide (lye) to it because it will contaminate the gallium.

 

[jasper]

hello really good content sir not a good chemistry background but just a question can we use p2p obtain form

Phenylacetone (P2P) synthesis via BMK ethyl glycidat and steam distillation​

in this method

 

[Consider]

Is this procedure verified, at times they will just post a procedure that is not real,

 

[idkyouthink]

I need a chemist in my lifee!!

 

[jasper]

Can we use methanol instead of ethanol or IPA

 

[Acidosis]

Yes

 

[Jordan Belfort]

IPA allows layering of the oil though, which means less boiling off/isolating.

Make sure you OVER use lye to neutralize the nitromethane because you will extract it. I personally suggest you use methanol, and hexane for extraction.

FITLER THE ALUFOIL off before adding lye because you get aluminium oxide in your hexane layer, impossible to clean unless you use celite or vacuum distill.

if you didn't use enough caustic the nitromethane will form an aezotrope with the freebase and distill it through your pumps.

only thing that could work, but yet have to try, extract with hexane if using methanol and acidfy with citric acid then distill off the nitromethane then freebase the oil again and distill.

 

[virus0815]

can sulfuric acid be replaced by hydrochloric acid?

 

[Jordan Belfort]

incase of starting the almgam you would want to add some sulfuric acid.

For crystallsation, yes you can use sulfuric acid if you want to smoke the sulfate but I suggest HCL.

 

[lalalander]

Can we convert the free base into methamphetamine hydrochloride with 37% hydrochloric acid? Also, in some videos, I have seen that the free base is converted directly into the hydrochloride salt with dry HCl gas, without the use of toluene. Why is that?